The goals of the experiment are to determine the chemical formulas for two hydrates through dehydration. Introduction: A chemical equation demonstrates the quantity of atoms of every component that make up the compound. The atomic proportion of components in the compound is the same as the molar proportion of those components. This information can be applied to solve for the mass of one mole of a compound by including the molar masses of the constituent components. Hydrates are combinations that are salts with water particles synthetically clung to them. Really, the holding is intriguing in that the water particles bond specifically to the metal cation. Hydrates fall in an expansive class called coordinated compounds in view of the sort …show more content…
A few metals can shape various hydrates. The item salt without water is called an anhydrate, If the masses of the hydrate and its subsequent anhydrate are measured, one can compute the molar proportion of water to salt and decide the hydrate's equation. Equations for hydrates are normally composed in the shape salt•xH2O, where x is the moles of water that stays with the salt. Procedure: 1. Determine the masses of the two empty crucibles. 2. We transferred the hydrates into their own crucibles. 3. We measured initially 5.7 grams of a Magnesium Sulfate Hydrate and 7.7 grams of a Zinc Sulfate Hydrate after subtracting the mass of the empty crucible. 4. With the crucible tongs, place the crucible and contents back on the clay triangle attached to the ring stand above the lit Bunsen burner. 5. We heated the hydrates in separate fume hoods with two Bunsen burners for ten minutes each. 6. We stopped heating the hydrates when they were within five percent measurements in three minute intervals after the first ten minutes. 7. Then the crucible tongs were used to remove the crucibles with their respective contents to record final masses of 2.8 grams of the Magnesium Sulfate Hydrate and 4.9 grams of the Zinc Sulfate Hydrate. 8. Clean up the lab area when finished with …show more content…
We could have possibly achieved our expected results if we had allowed the Zinc Sulfate Hydrate to cool down for those extra four minutes. The experimental error in this lab included the question whether the digital scale was as precise as it could be, how the cooling time affected the water in the hydrates, and any miscalculations that could have occurred. The digital scale could have been more precise since they are more precise scales that could deliver more accurate masses in this lab. The cooling time caused error when calculating the moles of water because the actual result was seven moles instead of five moles which was what was calculated. The calculations could have been potentially miscalculated particularly due to the significant figures used in the data. The method for this experiment can be improved by maybe using another object rather than the crucible to allow a faster cooling time that way the calculations for the analysis have less of a chance of
A hydrate is a compound that is bonded with a certain number of water molecules. When heated, the water will be driven out, thus being left with an anhydrate. The anhydrate is the hydrate minus the water. The hydrate must be
This experiment is based on determining the chemical formula for a hydrated compound containing copper, chloride, and water molecules in the crystal structure of the solid compound, using law of definite proportion. The general formula of the compound is CuxCly•zH2O, and aim is to determine chemical formula of this compound.
As a group, we obtained our salt mixture of calcium chloride and potassium oxalate, and weighed the mixture. We were able to make an aqueous solution from the mixture and distilled water. We boiled and filtered off the solution, leaving the precipitate. Once the precipitate was dried overnight, it was weighed and the mass was measured. Then we calculated the moles of the precipitate.
There are several sources of error to this experiment due to random and systematic errors. The only source of random error was the measurement that we took through the graduated cylinder which was only accurate to the nearest 1%. We took the largest error from this one percent, which was +/- 3. The largest relative error this yielded was only 3%, so this did not affect how precise this experiment was too much. We can still make this more precise by making the masses of the water larger. For example if we started the masses at 300mL and went up by 50mL, the largest error this would yield would be 2% due to the largest error being +/- 5. This would cause smaller errors in the amount of water.
29. When the thermometer reads 40°C, carry the beaker out of the heating apparatus with a beaker tong.
One possible source of error that can affect the results was that a mercury thermometer was used instead of an electronic one. The use of a mercury
At the beginning of the lab, the crucible is heated. What is the purpose of this step? How would your results (mole ratio of anhydride to water) have changed if you did not pre-heat the crucible? Explain. Feel free to use real numbers to
5. I believe that with a Bunsen burner to dry would have provided more accurate results for the hydration number because the heat can be applied more directly and the time to heat would be faster, giving less room for error in the
Place the beaker on the hot plate, place the thermometer in the beaker and set the hot plate to 5oC.
9) Trial E: Remove the syringe and empty the beaker. Add a Thermometer to the beaker. Add 200 mL of Room Temperature water to the beaker and heat with a Bunsen Burner until it reaches 100° C. Remove the Bunsen Burner. Repeat Steps 5 & 6.
The initial magnesium had a mass of 0.06 g while the final compound had a mass of 0.08 g. Magnesium oxide had been formed, and no magnesium should have been lost over the process due to magnesium being unable to form gases or liquids with any of the elements it had been exposed to.
A hydrate is a chemical compound containing salt and water. Depending on the salt, there is a maximum amount of water molecules that can be absorbed by the salt. An anhydrous salt is when the hydrate loses water, which happens when the hydrate is heated
The powdered cobalt oxalate hydrate was weighed to about 0.3 g and placed in a pre-weighed crucible. The crucible and the cobalt oxalate were then heated until the cobalt oxalate decomposed into a stable, black solid, or Co3O4. Once the crucible was sufficiently
Subsequently, two porcelain crucibles were used, weighed, and heated for about 10 minutes and then placed into a desiccator to cool. The two empty porcelain crucibles were first heated because the heat would vaporize any impurities that were originally on the crucible. The first crucible weighed 11.9047 g and the second crucible weighed 12.3735 g. Once the mass of the two crucibles
In this experiment, a saturated calcium sulfate was already made and ready to use. 25.00 mL of this solution was then mixed with 10 mL of an ammonia buffer and 1 drop of