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- A K2SO4 solution is prepared by weighing out a certain amount of the pure solid reagent,dissolving it to 500.0 mL in a volumetric flask. An aliquot was taken from this solution.of 25.00 ml and diluted to 500.0 ml. An aliquot of 5.00 was taken from this new solution anddiluted to 50.00 ml. A chemical analysis of this new solution showed a 0.100%(w/v)in K+. Calculate the weight of the pure solid K2SO4 used for the preparation of the original solution.and its concentration in each volumetric flask. The answer is 2.23x10^2g2. State the processes that can be adopted to purify and test the purity of sodium benzoateWhat is precipitation from homogeneous solution; what are the benefits of this method.
- Give a fundamental description of the recrystallization process. Explain why it is required and how it can be executed.3. Describe the characteristics that a crystal obtained through recrystallization must have, the final crystal, not the solvent.Briefly explain the principles involved in the separation of the components of a mixture by solvent extraction.
- 6 Assuming that hexane and water obey the required solubility criteria, why could they still not be used as a solvent pair in a mixed solvent recrystallization? Explain.4.Discussed the Purposed of the Golden rules in the practice of Forensic Chrmistry.How will the calculated molarity of the solution be affected if solid particles splatter out of the flask during the drying process? Explain. How will the calculated molarity be affected if the solute residue is not dried thoroughly? Explain.
- The solubility of water in diethyl ether has been reported to be 1.468 % by mass.' Assuming that 23.0 mL of diethyl ether were allowed to become saturated with water before used, and that the 1.2 g magnesium was the limiting reagent, what percentage of the product is expected to be lost due to the water in the solvent if the ether is not anhydrous?1,4‐Dimethoxybenzene (0.642 g) was dissolved in 2.0 mL acetic acid in a 25 mL Erlenmeyer flask using heat from a hot plate. Once the solid dissolved, 1.0 mL tert‐ butanol was added, and the reaction mixture was cooled in an ice bath. Then 2.0 mL concentrated sulfuric acid was added in 2‐3 drop portions,stirring the mixture after each aliquot. After the addition, the flask was removed from the ice bath and allowed to sit at room temperature for 15 minutes. Then 1.0 mL water was added dropwise to dilute the acid and the reaction mixture was added to 40 mL cold water in a 100 mL beaker. The solid was vacuum filtered and washed with 5 mL cold water, giving 52 g filtrate. The product wasrecrystallized from 4.5 mL methanol, yielding 0.317 g purified 1,4‐di‐tert‐butyl‐2,5‐dimethoxy benzene (27.2% yield). What is the atom economy, e-factor, and effective mass yield?A mixture of the two compounds shown below is dissolved in ether. Using the information given in the experiment, select all the correct statements regarding the extraction and isolation of the two compounds. lose 0000 X OH A. X can be extracted from the organic layer using sodium hydroxide. B. Y can precipitate out of the aqueous layer by the addition of sodium hydroxide to the salt of Y. C. X can precipitate out of the aqueous layer by the addition of sodium hydroxide to the salt of X. D. Y can be extracted from the organic layer using sodium hydroxide.