4000 100 80 60 IR Spectrum (liquid film) 20 % of base peak 40 3000 13C NMR Spectrum (100.0 MHz, CDCI, solution) Broton decoupled 10 DEPT CH₂ CH₂ CH you 200 80 1 9 1H NMR Spectrum (400 MHz, CDCI, solution) 8 2251 2000 v (cm¹) M = 117 120 160 m/e expansion 130 129 ppm expansion 130 129 ppm 160 1600 7 m 200 120 6 1200 Mass Spectrum 800 240 5 CgH7N 280 solvent 1 80 4 1 3 40 L 2 08 (ppm) 1 TMS L 0 8 (ppm)

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter19: Nuclear Magnetic Resonance Spectroscopy
Section: Chapter Questions
Problem 19.33QAP
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Using all the information provided come up with the structure of the compound

بیللا
4000
100
80
IR Spectrum
(liquid film)
60
40
20
% of base peak
40
3000
13C NMR Spectrum
(100.0 MHz, CDCI, solution)
10
DEPT CH₂ CH₂ CH
Proton decoupled
80
9
200
1H NMR Spectrum
(400 MHz, CDCI, solution)
1
2251
91
8
2000
120
M+ = 117
yu
v (cm¹)
160 200
m/e
expansion
130 129 ppm
expansion
130 129 ppm
160
1600
7
120
6
1200
Mass Spectrum
800
01
240 280
5
C8H7N
solvent
1
80
4
3
40
2
08 (ppm)
1
TMS
L
0
8 (ppm)
Transcribed Image Text:بیللا 4000 100 80 IR Spectrum (liquid film) 60 40 20 % of base peak 40 3000 13C NMR Spectrum (100.0 MHz, CDCI, solution) 10 DEPT CH₂ CH₂ CH Proton decoupled 80 9 200 1H NMR Spectrum (400 MHz, CDCI, solution) 1 2251 91 8 2000 120 M+ = 117 yu v (cm¹) 160 200 m/e expansion 130 129 ppm expansion 130 129 ppm 160 1600 7 120 6 1200 Mass Spectrum 800 01 240 280 5 C8H7N solvent 1 80 4 3 40 2 08 (ppm) 1 TMS L 0 8 (ppm)
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