A 0.500g sample is analyzed spectrophotometrically for manganese by dissolving it in acid and transferring to a 250 mL flask and diluting to volume. Three aliquots ae analyzed by transferring 50 mL portions with a pipet to 500 mL Erlenmeyer flask and reacting with an oxidizing agent, potassium peroxydisulfate, to convert the manganese to permanganate. After reaction, these are quantitatively transferred to 250 mL volumetric flasks, diluted to volume and measured spectrophotometrically. By comparison with standards, the average concentration of the final solution is determined to be 1.25 x 10^-5M. What is the percent manganese in the sample?

Fundamentals Of Analytical Chemistry
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ISBN:9781285640686
Author:Skoog
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Chapter13: Titrations In Analytical Chemistry
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A 0.500g sample is analyzed spectrophotometrically for manganese by dissolving it in acid and transferring to a 250 mL flask and diluting to volume. Three aliquots ae analyzed by transferring 50 mL portions with a pipet to 500 mL Erlenmeyer flask and reacting with an oxidizing agent, potassium peroxydisulfate, to convert the manganese to permanganate. After reaction, these are quantitatively transferred to 250 mL volumetric flasks, diluted to volume and measured spectrophotometrically.

By comparison with standards, the average concentration of the final solution is determined to be 1.25 x 10^-5M. What is the percent manganese in the sample?

for preparing the working standards.
36. A 0.500-g sample is analyzed spectrophotometrically for manganese by dissolving it in acid
and transferring to a 250-mL flask and diluting to volume. Three aliquots are analyzed by
transferring 50-mL portions with a pipet to 500-mL Erlenmeyer flasks and reacting with an
oxidizing agent, potassium peroxydisulfate, to convert the manganese to permanganate. After
reaction, these are quantitatively transferred to 250-mL volumetric flasks, diluted to volume,
and measured spectrophotometrically. By comparison with standards, the average concentration
in the final solution is determined to be 1.25 x 10 M. What is the percent manganese in the
sample?
Transcribed Image Text:for preparing the working standards. 36. A 0.500-g sample is analyzed spectrophotometrically for manganese by dissolving it in acid and transferring to a 250-mL flask and diluting to volume. Three aliquots are analyzed by transferring 50-mL portions with a pipet to 500-mL Erlenmeyer flasks and reacting with an oxidizing agent, potassium peroxydisulfate, to convert the manganese to permanganate. After reaction, these are quantitatively transferred to 250-mL volumetric flasks, diluted to volume, and measured spectrophotometrically. By comparison with standards, the average concentration in the final solution is determined to be 1.25 x 10 M. What is the percent manganese in the sample?
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