The following data were obtained from the calibration of an air-displacement pipette by repetitive drawing 1000.0 microliters of pure water at 4.00 °C using this pipette and weighing them on an analytical balance, which gave the following readings, respectively: 1.003, 1.000, 1.005, 1.007 g. How many measurements would have to be averaged to obtain an S/N of 1000? Type your numeric answer and submit
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![The following data were obtained from the calibration of an air-displacement pipette by repetitive
drawing 1000.0 microliters of pure water at 4.00 °C using this pipette and weighing them on an
analytical balance, which gave the following readings, respectively: 1.003, 1.000, 1.005, 1.007 g. How
many measurements would have to be averaged to obtain an S/N of 1000?
Type your numeric answer and submit](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2F2b8af10a-ad98-40ee-8aea-bd0ddab5fd56%2F29e7eb63-ddfe-417b-81ee-24a8cc84811f%2Fcnxzfu8_processed.jpeg&w=3840&q=75)
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- 2 (1) When performing chemical measurements, replicate experiments are often needed. This is to mitigate (Systematic or Random) error. (2) A CHEM 215 student performed 5 measurements of the wt% of SO4²- of a solid power sample. The results are 8.75%, 8.85%, 8.89%, 8.71%, 8.64%. The standard deviation is 0.10%. What is the confidence interval for this student's experiment at 95% confidence level. The t values for 95% confidence for degree of freedom from 1 to 5 are 12.71, 4.303, 3.182, 2.776, 2.571, respectively. Show your work!A potassium hydrogen phthalate solution was prepared by adding 0.0996 g of dry potassium hydrogen phthalate (MW = 204.22) in 100 mL distilled water. 1 mL of the prepared potassium hydrogen phthalate solution was transferred using pipette into 500-10000 mg/L COD tube before digested in the thermo-reactor at 148 oC for two hours. Calculate the measured COD reading in mg 02/L from the spectrophotometer at 600 nm if given oxygen molecular weight is 32 and the chemical equation for the oxidation reaction between potassium hydrogen phthalate (C8H5KO4) and chromic acid in the COD reagent tube is as follows: C8H5KO4 + 15/202 + H+ →→ 8C02 +K+ + 3H2O. (Note: MW is molecular weight)(2) A CHEM 215 student performed 5 measurements of the wt% of SO4²- of a solid power sample. The results are 8.75%, 8.85%, 8.89%, 8.71%, 8.64%. The standard deviation is 0.10%. What is the confidence interval for this student's experiment at 95% confidence level. The t values for 95% confidence for degree of freedom from 1 to 5 are 12.71, 4.303, 3.182, 2.776, 2.571, respectively. Show your work!
- The researcher extracts a sample of well water and prepares it for TXRF analysis with a 10.00 mg/L V internal standard, like the calibration standards. The result produces SCa = 69297.81 and SV = 13481.2.Determine the concentration of Ca.An atomic absorption method for the determination of the amount of iron present in used jet engine oil was found from pooling 30 triplicate analyses to have a standard deviation s = 3.1 µg Fe/mL. If s is a good estimate of o, calculate the 95 and 99% confidence intervals for the result 21.7 µg Fe/mL if it was based on the following criteria. (a) a single analysis 95% confidence interval= 21.7 + 99% confidence interval = 21.7 + (b) the mean of two analyses 95% confidence interval = 21.7 + 99% confidence interval= (c) the mean of six analyses 21.7 ± 95% confidence interval = 21.7 + 99% confidence interval= 21.7 + μg Fe/mL μg Fe/mL μg Fe/mL μg Fe/mL μg Fe/mL μg Fe/mLAn atomic absorption method for determination of copper in fuel samples yielded a pooled standard devia- tion of spooled = 0.27 µg Cu/mL (s). The analysis of an oil from a reciprocating aircraft engine showed a copper content of 7.91 µg Cu/mL. Calculate the 95 and 99% confidence intervals for the result if it was based on (a) a single analysis, (b) the mean of 4 analyses, and (c) the mean of 16 analyses.
- An atomic absorption method for the determination of the amount of iron present in used jet engine oil was found from pooling 30 triplicate analyses to have a standard deviation s = 3.6 mg Fe/mL. If s is a good estimate of σ, calculate the 95 and 99% confidence intervals for the result 18.5 mg Fe/mL if it was based on (a) a single analysis, (b) the mean of two analyses, and (c) the mean of four analyses.(5) If 200 g of polymer A, 300 g of polymer B, 500 g polymer C, and 100 g of polymer D are mixed, calculate both M, and Mw of the blend? Polymer A Mn = 45,000; Polymer B M, = 100,000; Mw = 200,000 Polymer C M, = 80,000; Polymer D What are the polydispersity index and the standard deviation of the number distribution of molecular weight of the mixture? Mw = 65,000 Mw = 85,000 Mn = 300,000; Mw = 900,000A standard method for analyzing aspirin tablets has a known variance of 20. A sample of 10 aspirin tablets is selected and analysed for the amount of aspirin using a modified method, yielding the following results: 254, 249, 252, 252, 249, 249, 250, 247, 251, 252. Determine whether the precision of the modified method is significantly different from that of the standard method at, alpha(a) = 0.10
- The Na* concentration in a blood serum sample was determined using the method of standard addition and atomic spectroscopy. 25.00 mL aliquots of serum were pipetted into five 50.00 mL volumetric flasks into which 2.640 M NaCl standard was added as shown in the table below. After dilution to volume, the emission of each solution was measured and used to plot a calibration graph. Flask 1 23 4 5 Vol. of standard (mL) 0 1.00 2.00 3.00 4.00 Emission signal 3.13 5.40 7.89 10.30 12.48 Analytical signal (emission) 14 42 10 12 4 2 0 0 0.05 y = 44.697x + 3.12 R² = 0.9995 0.1 0.15 Concentration of added analyte (M) 0.2 a) Using the plotted calibration graph, calculate the Na* concentration in the blood serum sample. b) Provide a possible reason why the serum sample might have been analysed using this analytical procedure. 0.25A unique plant was discovered from the hot springs of Maquinit, Coron, Palawan. To study the activity of the plant, approximately 5.00 g of the fresh plant was finely cut and ground and then mixed with an extraction buffer to make up a total of 1.00 mL crude plant extract. Approximately 19.00 mL of water was added to the plant extract. To determine the protein concentration of the extract, a bovine serum albumin (BSA) stock solution with a concentration of 200 ug mL-1 was used and mixtures with the following compositions and absorbance readings were prepared: A 200 uL aliquot of the diluted plant extract was added with 300 uL water and was subjected to Bradford assay. Determine the protein concentration, in mg mL-1, of the original 1.00 mL crude extract if the absorbance acquired from the analysis is 0.200.Suppose that something had gone "wrong" in the Big Bang and, instead of ordinary hydrogen, there was an abundance of deuterium in the Universe. There would be many subtle changes in equilibria, particularly the deuteron transfer equilibria of heavy acids and bases. The Kw for D20, at 25 °C, is 1.35 x 10-15. Calculate the pD and pOD in neutral heavy water at 25 °C. Ans: 7.45
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