ompounds 2,4 Dinitrophenylhydrazones Mix 2.5 mL of 2,4-dinitrophenylhydrazine in phosphoric acid and 25 mg of the unknown. Warm in a water bath for 5 min and let crystallization proceed. Collect the product by suction filtration and wash the crystals with cold water. Recrystallize from ethanol and let it dry until next time. NHÁNH, N-NH- -NO₂ R☑ R✗ R' NO₂ R' O₂N
ompounds 2,4 Dinitrophenylhydrazones Mix 2.5 mL of 2,4-dinitrophenylhydrazine in phosphoric acid and 25 mg of the unknown. Warm in a water bath for 5 min and let crystallization proceed. Collect the product by suction filtration and wash the crystals with cold water. Recrystallize from ethanol and let it dry until next time. NHÁNH, N-NH- -NO₂ R☑ R✗ R' NO₂ R' O₂N
Macroscale and Microscale Organic Experiments
7th Edition
ISBN:9781305577190
Author:Kenneth L. Williamson, Katherine M. Masters
Publisher:Kenneth L. Williamson, Katherine M. Masters
Chapter4: Recrystallization
Section: Chapter Questions
Problem 1Q
Related questions
Question
Please provide a mechanism for 2,4 dinitrophenylhydrazones reaction. The unknown is 3-pentanone. Please provide a mechanism for the reagents being added 3-pentanone.
![ompounds
2,4 Dinitrophenylhydrazones
Mix 2.5 mL of 2,4-dinitrophenylhydrazine in phosphoric
acid and 25 mg of the unknown. Warm in a water bath for 5
min and let crystallization proceed. Collect the product by
suction filtration and wash the crystals with cold water.
Recrystallize from ethanol and let it dry until next time.
NHÁNH,
N-NH-
-NO₂
R☑
R✗
R'
NO₂
R' O₂N](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2Fec2e8246-b7e6-4d22-a874-f5967d8173f8%2Fa811e44c-6a99-41d9-bceb-87e7e65b3ff9%2F8boe8rw_processed.png&w=3840&q=75)
Transcribed Image Text:ompounds
2,4 Dinitrophenylhydrazones
Mix 2.5 mL of 2,4-dinitrophenylhydrazine in phosphoric
acid and 25 mg of the unknown. Warm in a water bath for 5
min and let crystallization proceed. Collect the product by
suction filtration and wash the crystals with cold water.
Recrystallize from ethanol and let it dry until next time.
NHÁNH,
N-NH-
-NO₂
R☑
R✗
R'
NO₂
R' O₂N
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